Chemistry Laboratory II

Paper Code: 
25CCHY 114
Credits: 
02
Contact Hours: 
60.00
Max. Marks: 
100.00
Objective: 

This course will enable the students to

learn about pH measurement, surface tension and viscosity measurement of liquid pH-metric titrations of acids and bases.

Course Outcomes: 

Course

Learning Outcome

(at course level)

Learning and Teaching Strategies

Assessment Strategies

Course Code

Course

title

 

25CCHY 114

 

 

Chemistry Laboratory II

(Practical)

 

CO17: Determine the percentage composition of non interacting systems by viscosity and surface tension method.

CO18: Interpret powder diffraction patterns and operate a pH meter for pH-based experiments.

CO19: Compile and report the results efficiently, and develop communications skills.

CO20: Contribute effectively in course-specific interaction.

Approach in teaching:

Power point presentation, laboratory instructions and demonstrations.

 

 

Learning activities for the students:

Peer learning, hands-on-learning, interpretation of data, record

writing and learning through virtual labs.

 

Conduction of experiments, lab records, viva voce.

 

 

 

Unit I: 

· Surface tension measurements

· Determine the surface tension by (i) drop number (ii) drop weight method.

· Study the variation of surface tension of detergent solutions with concentration.

 

· Viscosity measurement using Ostwald’s viscometer

· Determination of viscosity of aqueous solutions of (i) polymer (ii) ethanol and (iii) sugar at room temperature.

· Study the variation of viscosity of sucrose solution with the concentration of solute.

 

· Indexing of a given powder diffraction pattern of a cubic crystalline system

 

· pH-metry

· Study the effect on pH of addition of HCl/NaOH to solutions of acetic acid, sodium acetate and their mixtures.

· Preparation of buffer solutions of different pH

· Sodium acetate-acetic acid

· Ammonium chloride-ammonium hydroxide

· pH metric titration of

· Strong acid vs strong base

· Weak acid vs strong base

· Determination of dissociation constant of a weak acid.

 

Any other experiment related to prescribed topic can be carried out in the class.

 

Essential Readings: 

1. Advanced Practical Physical Chemistry, Eighteenth Edition; J.B. Yadav; Goel Publishing House, Meerut, 2015.

2. Advanced University Practical Chemistry, Part I, First Edition; P.C. Kamboj, Vishal Publishing House, New Delhi; 2016.

 

References: 

1. Experimental Physical Chemistry; First Edition; V. D. Athawale, P. Mathur; New Age International (P) Ltd. Publishers, New Delhi, 2011.

2. Experiments in Physical Chemistry; Eight Edition; J.W. Nibler, & D. P. Shoemaker; McGraw-Hill: New York, 2003.

 

e-Resources:

1. https://www.fpharm.uniba.sk/fileadmin/faf/Pracoviska-subory/KFCHL/ENG/lectures/Physics/ AP11__Surface_tension.pdf (surface tension)

2. https://vlab.amrita.edu/index.php?sub=2&brch=190&sim=339&cnt=1 (viscosity)

3. https://chemcollective.org/chem/jsvlab/(pH-metry)

Academic Year: